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3-Chloro-2-methylaniline → N-(p-chlorobenzylidene)-2-methyl-3-chloroaniline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Chloro-2-methylaniline | HCID 6894 | — |
| 反応物 | 4-Chlorobenzaldehyde | HCID 7726 | — |
| 生成物 | N-(p-chlorobenzylidene)-2-methyl-3-chloroaniline | HCID 13017553 | — |
反応手順
2-methyl-3-chloroaniline (0.25 mole) and 4-chlorobenzaldehyde (0.25 mole) are ground in a mortar. The mixture is heated, with stirring in a water bath for 1.5 hours. Distillation at reduced pressure gives N-(p-chlorobenzylidene)-2-methyl-3-chloroaniline; Bp. 139° C./0/020 mm.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04152452 |
| 出典データセット | uspto-grants-1979_05 |
| ORD ID | ord-1440b92d0377440f9c15e6bd3a2a2ab7 |
| 出典メモ | uspto-grants-1979_05 |