HuagongsheHuagongshe Chemistry Print Report · For research reference only
alpha,alpha-Bis(p-chlorophenyl)-1-(methoxymethyl)imidazole-2-methanol → Bis-(4-chloro-phenyl)-(1H-imidazol-2-yl)-methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | alpha,alpha-Bis(p-chlorophenyl)-1-(methoxymethyl)imidazole-2-methanol | HCID 12433908 | — |
| Reactant | 1-[(Benzyloxy)methyl]-alpha-(p-chlorophenyl)-alpha-phenylimidazole-2-methanol | HCID 12433915 | — |
| Product | Bis-(4-chloro-phenyl)-(1H-imidazol-2-yl)-methanol | HCID 12433870 | — |
Reaction Steps
Using the procedure described in Example VIC but substituting an equivalent amount of α,α-bis(p-chlorophenyl)-1-(methoxymethyl)imidazole-2-methanol for the 1-[(benzyloxy)methyl]-α-(p-chlorophenyl)-α-phenylimidazole-2-methanol, α,α-bis(p-chlorophenyl)imidazole-2-methanol was obtained. Melting point of the product was 195°-197° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04152441 |
| Source dataset | uspto-grants-1979_05 |
| ORD ID | ord-6e743dc9e02f4c939693f55e79f1055f |
| Source note | uspto-grants-1979_05 |