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alpha-(p-Fluorophenyl)-1-(methoxymethyl)-alpha-phenylimidazole-2-methanol → (4-fluorophenyl)(1H-imidazol-2-yl)phenylmethanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | alpha-(p-Fluorophenyl)-1-(methoxymethyl)-alpha-phenylimidazole-2-methanol | HCID 12433900 | — |
| 反応物 | 1-[(Benzyloxy)methyl]-alpha-(p-chlorophenyl)-alpha-phenylimidazole-2-methanol | HCID 12433915 | — |
| 生成物 | (4-fluorophenyl)(1H-imidazol-2-yl)phenylmethanol | HCID 12433859 | — |
反応手順
Using the procedure described in Example VIC but substituting an equivalent amount of α-(p-fluorophenyl)-1-(methoxymethyl)-α-phenylimidazole-2-methanol for the 1-[(benzyloxy)methyl]-α-(p-chlorophenyl)-α-phenylimidazole-2-methanol, α-(p-fluorophenyl)-α-phenylimidazole-2-methanol was obtained. Its melting point was 199-200.5° C. after crystallisation from acetone.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04152441 |
| 出典データセット | uspto-grants-1979_05 |
| ORD ID | ord-f00974106be14930821331b38229f7b6 |
| 出典メモ | uspto-grants-1979_05 |