huagongshe.com
HRID261955

反应详情

EQUATION

反应方程式

HRID 261955 的结构方程式

REACTANTS

反应物

4
结构：CN(C)CCN(C)C
HCID8037

N,N,N',N'-Tetramethylethylenediamine

C6H16N2

结构：C=Cn1ccnc1
HCID66171

1-Vinylimidazole

C5H6N2

结构：CC(C)(C)c1ccc(C(=O)c2ccc(C(C)(C)C)cc2)cc1
HCID2758048

Bis(4-tert-butylphenyl)methanone

C21H26O

结构：[Li]CCCC
HCID178418339

未命名化合物

PRODUCTS

生成物

1
结构：C=Cn1ccnc1C(O)(c1ccc(C(C)(C)C)cc1)c1ccc(C(C)(C)C)cc1
HCID12433927

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCCCCC
溶剂HCID8058

n-Hexane

C6H14

PROCEDURE

实验过程

This compound was prepared by the procedure indicated in Example XXII A, using the following materials: 10 g. (0.03 mol) of 4,4'-di-tert.-butylbenzophenone, 19.5 ml. (0.04 mol) of 20% butyllithium in n-hexane, 3 g. (0.03 mol) of 1-vinylimidazole and 4.9 g. (0.04 mol) of N,N,N', N'-tetramethylethylenediamine. The product was crystallised from ethyl acetate. Melting point 169°-170° C.

WORKUP

后处理

  1. customThis compound was prepared by the procedure
  2. customThe product was crystallised from ethyl acetate