HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → 1,1-Dimethoxy-3-(methylthio)propane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | Methional | HCID 18635 | — |
| Product | 1,1-Dimethoxy-3-(methylthio)propane | HCID 83240 | — |
Reaction Steps
20.8 g (0.2 mole) of freshly distilled methional and 100 cc of methyl alcohol are heated under reflux in the presence of 0.5 g of p-toluene sulphonic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04153442 |
| Source dataset | uspto-grants-1979_05 |
| ORD ID | ord-05cd24cd39d3416fa9ff0929ffee6348 |
| Source note | uspto-grants-1979_05 |