Ethanolamine → HCID 21320082, compound

HRID 262115Notes

Reaction equation

HRID 262115 reaction equation
OCCN.Cl.C1([CH:12]2[CH2:22][N:15]3[C:16]([CH3:21])=[N:17][C:18]([Cl:20])=[CH:19][C:14]3=[N:13]2)C=CC=CC=1>>[CH3:21][C:16]1[N:15]2[CH2:22][CH2:12][N:13]=[C:14]2[CH:19]=[C:18]([Cl:20])[N:17]=1

Participants

3

Reactant 2

HCID 700EthanolamineHCID 21320113HCID 21320113, compound

Product 1

HCID 21320082HCID 21320082, compound

Procedure

By substituting α-phenyl-β-hydroxyethylamine for β-hydroxyethylamine in the above procedure, 2-phenyl-5-methyl-7-chloro-2,3-dihydroimidazo[1,2-c]pyrimidine hydrochloride was prepared decomposing about 150° C. after recrystallization from an ethanol-ethyl acetate ether solvent mixture.

Workup

  1. customwas prepared
  2. customdecomposing about 150° C.
  3. customafter recrystallization from an ethanol-ethyl acetate ether solvent mixture

Sources & evidence

ORD record
ord-920e3448475f4531b94775f0961f0248
Source dataset
uspto-grants-1979_05
Patent number
US04153695

Reaction notes

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