N-bromobutanimide → HCID 53899085, compound

HRID 262203Notes

Reaction equation

HRID 262203 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]=[CH:9][C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)=[CH:4][CH:3]=1.[Br:16]N1C(=O)CCC1=O>C(Cl)(Cl)(Cl)Cl>[CH:8]([C:5]1[CH:6]=[CH:7][C:2]([CH2:1][Br:16])=[CH:3][CH:4]=1)=[CH:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1

Participants

4

Reactant 2

HCID 67184N-bromobutanimideHCID 296657HCID 296657, compound

Product 1

HCID 53899085HCID 53899085, compound

Reagents, catalysts & solvents 1

HCID 5943Carbon TetrachlorideSolvent

Procedure

4-Styrylbenzyl bromide was prepared from 35.4 g. of 4-methylstilbene and 35.6 g. of N-bromosuccinimide in carbon tetrachloride according to the procedure of Example 8(a); yield 35.5 g., m.p. 125°-127° C. after recrystallization from benzene-cyclohexane and acetonitrile.

Workup

  1. custom, m.p. 125°-127° C. after recrystallization from benzene-cyclohexane and acetonitrile

Sources & evidence

ORD record
ord-b84a5458532b405385499e656d493b97
Source dataset
uspto-grants-1979_05
Patent number
US04153719

Reaction notes

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