HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron trifluoride etherate → 3-(4-Chlorophenyl)-2,3-dihydro-1H-indole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron trifluoride etherate | HCID 8000 | — |
| Reactant | 3-(4-Chlorophenyl)-1H-indole | HCID 15322479 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 3-(4-Chlorophenyl)-2,3-dihydro-1H-indole | HCID 53732316 | — |
Reaction Steps
Using the same procedure as detailed in Example 1 3.5 g of 3-p-chlorophenylindole, 35 ml of glacial acetic acid, 7 ml of boron trifluoride etherate and 7 g of zinc dust were reacted together and the product worked up as in Example 1. In this way 1.5 g of the desired 3-p-chlorophenylindoline was obtained as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04153789 |
| Source dataset | uspto-grants-1979_05 |
| ORD ID | ord-463c4a091e8d4946bd3905f90794be79 |
| Source note | uspto-grants-1979_05 |