Methanamine, N-methoxy-, hydrochloride (1:1) → HCID 21318679, compound

HRID 262408Notes

Reaction equation

HRID 262408 reaction equation
[S:1]1[CH:5]=[CH:4][C:3]2[CH2:6][CH2:7][CH2:8][CH:9]([N:10]=[C:11]=[S:12])[C:2]1=2.Cl.[CH3:14][O:15][NH:16][CH3:17]>>[CH3:17][N:16]([O:15][CH3:14])[C:11]([NH:10][CH:9]1[C:2]2[S:1][CH:5]=[CH:4][C:3]=2[CH2:6][CH2:7][CH2:8]1)=[S:12]

Participants

3

Reactant 2

HCID 81138Methanamine, N-methoxy-, hydrochloride (1:1)HCID 21318675HCID 21318675, compound

Product 1

HCID 21318679HCID 21318679, compound

Procedure

In the manner described in Example 5, 4,5,6,7-tetrahydrobenzo[b]thien-7-yl isothiocyanate is allowed to react with O,N-dimethylhydroxylamine hydrochloride to afford the title compound.

Sources & evidence

ORD record
ord-21dd74082dc64ae9b6f4c9848b43ed97
Source dataset
uspto-grants-1979_05
Patent number
US04154740

Reaction notes

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