HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 13015402, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 13015401 | HCID 13015401 | — |
| Product | HCID 13015402 | HCID 13015402 | — |
Reaction Steps
The above reaction is repeated on 12.3 g. of 5-trichlorovinyl pyridine-2-carboxylic acid and 145 ml. of thionyl chloride affording a tan solid with a m.p. 89°-90° C. The crude 5-trichlorovinyl pyridine-2-carboxylic acid chloride are used without further purification in subsequent steps.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04154835 |
| Source dataset | uspto-grants-1979_05 |
| ORD ID | ord-ba49dd19c61a4b58828ac537249616f4 |
| Source note | uspto-grants-1979_05 |