HuagongsheHuagongshe Chemistry Print Report · For research reference only
ethyl (2Z)-3-(pyridin-3-yl)but-2-enoate → HCID 12727116, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | ethyl (2Z)-3-(pyridin-3-yl)but-2-enoate | HCID 67402107 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12727116 | HCID 12727116 | — |
Reaction Steps
Ethyl 3-(3-pyridyl)crotonate (prepared from treating 3-acetylpyridine with ethoxycarbonylmethyltriphenylphosphonium bromide and sodium ethoxide) was hydrogenated in ethanol at 40 p.s.i. with 10% palladium on charcoal catalyst to give ethyl 3-(3-pyridyl)butyrate, b.p. 74° /0.15 mmHg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04154834 |
| Source dataset | uspto-grants-1979_05 |
| ORD ID | ord-2cf90d1d47c149628cb15abf2a1798c1 |
| Source note | uspto-grants-1979_05 |