HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzhydrol → 1-[3-[(diphenylmethyl)thio]-2-benzylpropanoyl]-L-proline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzhydrol | HCID 7037 | — |
| Reactant | 1-[3-Phenyl-2-(sulfanylmethyl)propanoyl]-L-proline | HCID 18397285 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | 1-[3-[(diphenylmethyl)thio]-2-benzylpropanoyl]-L-proline | HCID 54380838 | — |
Reaction Steps
Diphenylmethanol (0.92 g) and 1-(3-mercapto-2-benzylpropanoyl)-L-proline (1.5 g) are dissolved in trifluoroacetic acid (10 ml) and the solution is kept at room temperature for 30 minutes. The excess trifluoroacetic acid is removed in vacuo to yield 1-[3-[(diphenylmethyl)thio]-2-benzylpropanoyl]-L-proline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04154840 |
| Source dataset | uspto-grants-1979_05 |
| ORD ID | ord-668bc1d4c09040be853dfc2d5b1471b0 |
| Source note | uspto-grants-1979_05 |