HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Formicin → 3-Acetamidomethylthio-2-methylpropanoic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Formicin | HCID 69365 | — |
| Edukt | 3-Mercaptoisobutyric acid | HCID 152910 | — |
| Lösungsmittel | Trifluoroacetic acid | HCID 6422 | — |
| Produkt | 3-Acetamidomethylthio-2-methylpropanoic acid | HCID 21319145 | — |
Reaktionsschritte
3-Mercapto-2-methylpropanoic acid (2.4 g.) and N-hydroxymethylacetamide (1.8 g.) are dissolved in trifluoroacetic acid and the solution is stored at room temperature for one hour. The trifluoroacetic acid is removed in vacuo and the residue is dried in vacuo over potassium hydroxide to yield 3-acetamidomethylthio-2-methylpropanoic acid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04154840 |
| Quelldatensatz | uspto-grants-1979_05 |
| ORD ID | ord-0608b8bc62914d75bd49bba4023019fe |
| Quellennotiz | uspto-grants-1979_05 |