HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Chloromethyl)phenylacetic acid → p-Sulfomethylphenylacetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Chloromethyl)phenylacetic acid | HCID 10313419 | — |
| Reactant | Sodium Bisulfite | HCID 23665763 | — |
| Product | p-Sulfomethylphenylacetic acid | HCID 23337711 | — |
Reaction Steps
To a boiling aqueous solution of sodium bisulfite (1.47 g, 0.0141 mole) is added in portions p-chloromethylphenylacetic acid (2.6 g, 0.0141 mole). The solution is further refluxed for 30 minutes and is then evaporated to dryness to give a quantitative yield of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04148997 |
| Source dataset | uspto-grants-1979_04 |
| ORD ID | ord-ca4477f096bc46d990edfe697841cf74 |
| Source note | uspto-grants-1979_04 |