HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 53916716, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Phenyl chloroformate | HCID 15891 | — |
| Reactant | HCID 54513359 | HCID 54513359 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 53916716 | HCID 53916716 | — |
Reaction Steps
A mixture of XXVI (0.01 m) from Step (a) above, 4 g potassium carbonate and phenylchloroformate (0.03 m) in 50 ml toluene is heated at reflux for 24 hours. The cooled reaction mixture is treated with water. The toluene layer is separated, dried (MgSO4), filtered and concentrated to give the title product as a crude oil used directly in the next reaction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04154932 |
| Source dataset | uspto-grants-1979_05 |
| ORD ID | ord-9e418fd6e8ef46d9badb0bba46ee11e6 |
| Source note | uspto-grants-1979_05 |