HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → HCID 54132427, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 54301983 | HCID 54301983 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 54132427 | HCID 54132427 | — |
Reaction Steps
A mixture of XXVIII (0.005 m) from Step (c) above, ethyl iodide (0.01 m) and potassium carbonate (2 g) in 20 ml acetonitrile is heated at reflux for 18 hours. The mixture is filtered and the filtrate concentrated. The residue is treated with water and extracted with methylene chloride. The extracts are dried (MgSO4), filtered and concentrated to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04154932 |
| Source dataset | uspto-grants-1979_05 |
| ORD ID | ord-aa9a657ab6f841b1b78b29842e7a923a |
| Source note | uspto-grants-1979_05 |