Sodium Sulfate → HCID 54212115, compound

Participants

Reaction Steps

The product of Step (c) (XXXIII) (0.005 m) in tetrahydrofuran (20 ml) is added to a suspension of lithium aluminum hydride (0.57 g) in tetrahydrofuran (20 ml), and the mixture is heated at reflux for 18 hours. The mixture is then cooled and saturated sodium sulfate solution (1.8 ml) and a few drops of dilute sodium hydroxide are cautiously added. The mixture is warmed until the solids are completely white. Solid sodium sulfate is added, the solids are removed by filtration and washed well with ethyl acetate. Concentration of the combined filtrate and washes gives the title product.

Provenance & Evidence