HCID 21318774, compound → HCID 21318797, compound
Reaction equation
[CH2:1]([NH:9][C:10]1[CH:23]=[CH:22][C:13]([C:14]([CH2:16][C:17]([O:19]CC)=[O:18])=[O:15])=[CH:12][CH:11]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[CH2:24]([NH:36][C:37]1[CH:50]=[CH:49][C:40]([C:41]([CH2:43][C:44]([O:46]CC)=[O:45])=[O:42])=[CH:39][CH:38]=1)[CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH3:35].[CH2:51]([NH:65][C:66]1[CH:79]=[CH:78][C:69]([C:70]([CH2:72][C:73]([O:75]CC)=[O:74])=[O:71])=[CH:68][CH:67]=1)[CH2:52][CH2:53][CH2:54][CH2:55][CH2:56][CH2:57][CH2:58][CH2:59][CH2:60][CH2:61][CH2:62][CH2:63][CH3:64]>>[CH2:1]([NH:9][C:10]1[CH:23]=[CH:22][C:13]([C:14]([CH2:16][C:17]([OH:19])=[O:18])=[O:15])=[CH:12][CH:11]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[CH2:24]([NH:36][C:37]1[CH:38]=[CH:39][C:40]([C:41]([CH2:43][C:44]([OH:46])=[O:45])=[O:42])=[CH:49][CH:50]=1)[CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH3:35].[CH2:51]([NH:65][C:66]1[CH:67]=[CH:68][C:69]([C:70]([CH2:72][C:73]([OH:75])=[O:74])=[O:71])=[CH:78][CH:79]=1)[CH2:52][CH2:53][CH2:54][CH2:55][CH2:56][CH2:57][CH2:58][CH2:59][CH2:60][CH2:61][CH2:62][CH2:63][CH3:64]Participants
6
Procedure
By employing an equimolar amount of ethyl p-(octylamino)benzoylacetate, ethyl p-(dodecylamino)benzoylacetate, ethyl p-(tetradecylamino)benzoylacetate, and ethyl p-(nonadecylamino)benzoyl acetate instead of the ethyl p-hexadecylaminobenzoyl acetate above, there is obtained p-octylaminobenzoylacetic acid, p-dodecylaminobenzoylacetic acid, p-tetradecylaminobenzoylacetic acid, and p-nonadecylaminoenzoylacetic acid, respectively.
Sources & evidence
- ORD record
- ord-2e7f389967af47239591329f38b01252
- Source dataset
- uspto-grants-1979_05
- Patent number
- US04154756
Reaction notes
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