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Nitrobenzene → 1,7-Dinitroanthraquinone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Nitrobenzene | HCID 7416 | — |
| 反応物 | 9,10-Anthracenedione, 1,2-dinitro- | HCID 42596 | — |
| 生成物 | 1,7-Dinitroanthraquinone | HCID 74147 | — |
反応手順
100 g of a dinitroanthraquinone mixture of the composition A are employed and are stirred with C ml of nitrobenzene at D° C. for B hours, the precipitate is filtered off at D° C. and washed with 50 ml of nitrobenzene and the material on the filter is freed from nitrobenzene in vacuo. E g of 1,7-dinitro-anthraquinone of the composition F are obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04155921 |
| 出典データセット | uspto-grants-1979_05 |
| ORD ID | ord-f4a79c98b0d146c1877b4b11d58141ec |
| 出典メモ | uspto-grants-1979_05 |