HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trichloroacetyl isocyanate → HCID 13047563, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trichloroacetyl isocyanate | HCID 76400 | — |
| Reactant | HCID 357307 | HCID 357307 | — |
| Product | HCID 13047563 | HCID 13047563 | 72.6% |
Reaction Steps
Following the procedure substantially the same as described in Example 1, Step C, 1.97 g of 4,6-dimethoxysalicylaldoxime is treated with 2.0 g of trichloroacetylisocyanate to yield 1.3 g (72.6%) of 4,6-dimethoxy-1,2-benzisoxazole, m.p. 100°-101° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04156005 |
| Source dataset | uspto-grants-1979_05 |
| ORD ID | ord-5fbe7a9b7aa6473ea5fb7b701ba14e20 |
| Source note | uspto-grants-1979_05 |