5-Chloro-2-nitroaniline → HCID 21318009, compound

Participants

Reaction Steps

To a solution of 6.9 g (0.04 mole) of 5-chloro-2-nitroaniline in 50 ml of absolute ethanol there is added 6.0 g of the potassium salt of 1-cyclohexene-1-thiol [J. Praktische Chemie 34, 116 (1966)]. The mixture is heated on the steam bath for 0.5 hour, filtered and the filtrate is reduced in volume in vacuo. The resulting solid is filtered off and crystallized from absolute ethanol to yield 5.3 g, m.p. 100°-102°.

Provenance & Evidence