Ethanolamine → HCID 54459075, compound

HRID 263072Notes

Reaction equation

HRID 263072 reaction equation
[Cl:1][C:2]1[CH:18]=[CH:17][C:5]([O:6][C:7]2[CH:12]=[CH:11][C:10]([CH2:13][C:14](O)=[S:15])=[CH:9][CH:8]=2)=[CH:4][CH:3]=1.[NH2:19][CH2:20][CH2:21][OH:22]>>[OH:22][CH2:21][CH2:20][NH:19][C:14](=[S:15])[CH2:13][C:10]1[CH:11]=[CH:12][C:7]([O:6][C:5]2[CH:17]=[CH:18][C:2]([Cl:1])=[CH:3][CH:4]=2)=[CH:8][CH:9]=1

Participants

3

Reactant 2

HCID 700EthanolamineHCID 178526163HCID 178526163, compound

Product 1

HCID 54459075HCID 54459075, compound

Procedure

On subjecting the acid of Example 10 to an amidification reaction with 2-amino-ethanol in accordance with the working method described in Example 7, CRL 40,272 is obtained.

Workup

  1. customCRL 40,272 is obtained

Sources & evidence

ORD record
ord-9fa0f5025fb34c4f8631992bfadd05a2
Source dataset
uspto-grants-1979_05
Patent number
US04156011

Reaction notes

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