Thionyl Chloride → HCID 21318074, compound

HRID 263091Notes

Reaction equation

HRID 263091 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([S:8][C:9]2[CH:21]=[CH:20][C:12]([O:13][C:14]([CH3:19])([CH3:18])[C:15](O)=[O:16])=[CH:11][CH:10]=2)=[CH:4][CH:3]=1.S(Cl)([Cl:24])=O>C1C=CC=CC=1>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([S:8][C:9]2[CH:21]=[CH:20][C:12]([O:13][C:14]([CH3:19])([CH3:18])[C:15]([Cl:24])=[O:16])=[CH:11][CH:10]=2)=[CH:4][CH:3]=1

Participants

4

Reactant 2

HCID 24386Thionyl ChlorideHCID 21318046HCID 21318046, compound

Product 1

HCID 21318074HCID 21318074, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

A mixture of 15 g (0.0465 mol) of p-(p-chlorophenylthio)-phenoxy-isobutyric acid (CRL 40,201) and of 16.75 ml (0.232 mol) of thionyl chloride is heated to the reflux temperature for 10 minutes. After having taken up the reaction mixture in benzene, filtered the solution in the presence of carbon black and evaporated the solvent, 16 g of an orange-coloured oil are obtained.

Workup

  1. filtrationfiltered the solution in the presence of carbon black
  2. customevaporated the solvent, 16 g of an orange-coloured oil
  3. customare obtained

Sources & evidence

ORD record
ord-3200b10d16f64416b7ab57feee729941
Source dataset
uspto-grants-1979_05
Patent number
US04156011

Reaction notes

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