Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Phenethylamine | HCID 1001 | — |
| Reactant | HCID 20298687 | HCID 20298687 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 20298673 | HCID 20298673 | 92.1% |
Reaction Steps
5-Methoxy-2-[3-(4-morpholinyl)propoxy]benzaldehyde (33.4 g) and 14.5 g of phenethylamine are refluxed in 120 ml of toluene for about 1 hour. After cooling to about 50° C., the solvent is removed using a rotary evaporator and the oily residue is distilled to give 42.1 g of the title compound, boiling point 240°-245° C. at 0.2-0.3 mm of Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04156079 |
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| Source dataset | uspto-grants-1979_05 |
|---|
| ORD ID | ord-38f81aca13684e9d9378d3dd571080cc |
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| Source note | uspto-grants-1979_05 |
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