HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenethylamine → N-[[3-Methoxy-2-[3-(4-morpholinyl)propoxy]phenyl]methylene]benzeneethanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenethylamine | HCID 1001 | — |
| Reactant | 3-Methoxy-2-[3-(4-morpholinyl)propoxy]benzaldehyde | HCID 2200348 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | N-[[3-Methoxy-2-[3-(4-morpholinyl)propoxy]phenyl]methylene]benzeneethanamine | HCID 20298672 | 85.9% |
Reaction Steps
3-Methoxy-2-[3-(4-morpholinyl)propoxy]benzaldehyde (42.5 g) and 18.5 g of phenethylamine are reacted in 150 ml of toluene following the procedure described in Example 1B, yielding 50.0 g of the title compound, boiling point 229°-234° C. at 0.2-0.3 mm of Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04156079 |
| Source dataset | uspto-grants-1979_05 |
| ORD ID | ord-7570d6d9087a47b5a8672c3631e77cdd |
| Source note | uspto-grants-1979_05 |