HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → 1-Acetyl-3,5-dipyrazinyl-1,2,4-triazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 2-(5-pyrazin-2-yl-4H-1,2,4-triazol-3-yl)pyrazine | HCID 13524787 | — |
| Product | 1-Acetyl-3,5-dipyrazinyl-1,2,4-triazole | HCID 20285816 | — |
Reaction Steps
A suspension of 3,5-dipyrazinyl-1,2,4-triazole (0.5 grams) in 20 ml. of acetic anhydride is heated on a steam bath for 17 hours. The resulting solution is filtered and concentrated to a solid. After recrystallization from benzene-hexane, 250 mg. of 1-acetyl-3,5-dipyrazinyl-1,2,4-triazole is obtained, m.p. 128°-130° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04156085 |
| Source dataset | uspto-grants-1979_05 |
| ORD ID | ord-2775615e289c488682e3d0d1c0f31256 |
| Source note | uspto-grants-1979_05 |