HuagongsheHuagongshe Chemistry Print Report · For research reference only
P-Anisidine → 2-Naphthalenecarboxamide, 4-amino-N-[4-[2,4-bis(1,1-dimethylpropyl)phenoxy]butyl]-1-hydroxy-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | P-Anisidine | HCID 7732 | — |
| Reactant | Sodium Dithionite | HCID 24489 | — |
| Reactant | 2-Naphthalenecarboxamide, N-[4-[2,4-bis(1,1-dimethylpropyl)phenoxy]butyl]-1-hydroxy- | HCID 122566 | — |
| Product | 2-Naphthalenecarboxamide, 4-amino-N-[4-[2,4-bis(1,1-dimethylpropyl)phenoxy]butyl]-1-hydroxy- | HCID 3084862 | — |
Reaction Steps
1-Hydroxy-N-[4-(2,4-di-t-pentylphenoxy)-butyl]-2-naphthamide was coupled with a diazotized p-anisidine ##STR29## The azo group of the compound thus prepared was then reduced with sodium dithionite (Na2S2O4) to the corresponding amine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04156609 |
| Source dataset | uspto-grants-1979_05 |
| ORD ID | ord-0aa4b877d78b4c20b4b0d20fc1f0e007 |
| Source note | uspto-grants-1979_05 |