HRID263209

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID14798

Sodium Hydroxide

HNaO

HCID23347795

4-Amino-5,6-dihydro-1-benzothiophen-7(4H)-one--hydrogen chloride (1/1)

C8H10ClNOS

PRODUCTS

生成物

HCID23347796

4-Amino-5,6-dihydro-1-benzothiophen-7(4H)-one

C8H9NOS

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID962

Water

H2O

PROCEDURE

实验过程

The free amine is obtained by neutralizing the amine hydrochloride in water with sodium hydroxide solution. It is separated by extraction with CHCl3 and removal of the CHCl3 in vacuo affords 4,5,6,7-tetrahydro-7-oxobenzo[b]thiophen-4-amine.

WORKUP

后处理

customIt is separated by extraction with CHCl3 and removal of the CHCl3 in vacuo