HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 70510436, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 70509255 | HCID 70509255 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 70510436 | HCID 70510436 | — |
Reaction Steps
1-Methylthio-1-[2-((3-methoxy-2-pyridyl)methylthio)ethylamino]-2-nitroethylene (1.4g) was stirred with a solution of methylamine in ethanol (25 ml, 33% solution) and dissolved within a minute. After a further 3 minutes a crystalline product separated and recrystallisation from ethanol/ether yielded the title product (1.1 g), m.p. 145.5°-147°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04156727 |
| Source dataset | uspto-grants-1979_05 |
| ORD ID | ord-2b622062de974479a8e455d6f17e5bbf |
| Source note | uspto-grants-1979_05 |