HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylenediamine → p-Toluenesulfonamide, N,N'-ethylenebis-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylenediamine | HCID 3301 | — |
| Reactant | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | p-Toluenesulfonamide, N,N'-ethylenebis- | HCID 95237 | — |
Reaction Steps
Treat ethylenediamine with p-toluenesulfonyl chloride (i.e. tosyl chloride) and sodium hydroxide in aqueous ether according to known procedures to obtain N,N'-ditosylethylenediamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04156683 |
| Source dataset | uspto-grants-1979_05 |
| ORD ID | ord-dda94c5143d2401197c1116a206ee9d3 |
| Source note | uspto-grants-1979_05 |