HRID263298

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID73817

3-Methylbenzo[b]thiophene

C9H8S

HCID3017979

4-Chloro-3-sulfamoylbenzoyl chloride

C7H5Cl2NO3S

HCID6451240

未命名化合物

PRODUCTS

生成物

结构：Cc1c(C(=O)c2ccc(Cl)c(S(N)(=O)=O)c2)sc2ccccc12

HCID21316639

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID7964

Chlorobenzene

C6H5Cl

PROCEDURE

实验过程

is obtained as described in Example 1 from 2.5 g 4-chloro-3-sulfamoylbenzoyl chloride, 1.6 g 3-methylbenzo[b]thiophene and 3 g aluminum chloride in 50 ml chlorobenzene. Colorless crystals, m.p. 210° C.

WORKUP

后处理

customis obtained