HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl bromoacetate → 4-(S)-Isopropyl-3-[2-(R)-tert-butoxycarbonylmethyl-1-oxononyl]-2-oxazolidinone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl bromoacetate | HCID 79177 | — |
| Reactant | 4-(S)-Isopropyl-3-(1-oxononyl)-2-oxazolidinone | HCID 10588060 | — |
| Product | 4-(S)-Isopropyl-3-[2-(R)-tert-butoxycarbonylmethyl-1-oxononyl]-2-oxazolidinone | HCID 10786208 | — |
Reaction Steps
Following the procedure described in Referential Example 4, but using 4-(S)-isopropyl-3-(1-oxononyl)-2-oxazolidinone (10.09 g), prepared in Referential Example 71, and tert-butyl bromoacetate (30 ml), the desired compound (12.62 g) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05643908 |
| Source dataset | uspto-grants-1997_07 |
| ORD ID | ord-5745abe5b81b46a0ae9ba550d92a5abd |
| Source note | uspto-grants-1997_07 |