HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cadmium chloride, dihydrate → 5-Chloro-2-methyl-3-isothiazolone cadmium(II)chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cadmium chloride, dihydrate | HCID 24633 | — |
| Reactant | 5-Chloro-2-methyl-4-isothiazolin-3-one | HCID 33344 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 5-Chloro-2-methyl-3-isothiazolone cadmium(II)chloride | HCID 86736469 | 200.3% |
Reaction Steps
To a solution of 5.5 g (0.03 mole) of anhydrous cadmium chloride in 120 ml of ethanol was added a solution of 4.5 g (0.03 mole) of 5-chloro-2-methyl-3-isothiazolone in 25 ml of ethanol. A white precipitate formed immediately. The mixture was filtered and air dried to yield 10.0 g (100%) of product, m.p. >250° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04150026 |
| Source dataset | uspto-grants-1979_04 |
| ORD ID | ord-37e4b18ce99e4f68b80c25279140ce72 |
| Source note | uspto-grants-1979_04 |