HRID263637

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CC1=C(CC(=O)O)c2cc(F)ccc2C1=Cc1ccc(S(C)(=O)=O)cc1

HCID114866

5-Fluoro-2-methyl-1-[[4-(methylsulfonyl)phenyl]methylene]-1H-indene-3-acetic acid

C20H17FO4S

HCID10942334

Methanol, sodium salt

CH3NaO

PRODUCTS

生成物

结构：CC1=C(CC(=O)[O-])c2cc(F)ccc2C1=Cc1ccc(S(C)(=O)=O)cc1.[Na+]

HCID70149782

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID887

Methanol

CH4O

2 次

PROCEDURE

实验过程

5-fluoro-2-methyl-1-(ρ-methylsulfonylbenzylidene)-3-indenylacetic acid (1.79 g.) in methanol (10 ml.) is added to a solution of sodium methoxide (0.27 g.) in methanol (5 ml.). The reaction mixture is stirred for 20 minutes and evaporated to dryness to yield sodium 5-fluoro-2-methyl-1-(ρ-methylsulfonylbenzylidene)-3-indenylacetate.

WORKUP

后处理

customevaporated to dryness