Hydrochloric Acid → HCID 18674686, compound

Participants

Reaction Steps

To a 4 g sample of product, 3-chloro-N-propyl-N-4-pyridinyl-1H-indol- 1 -amine, dissolved in anhydrous ether (60 mL) in a 125 mL-round bottom flask equipped with a mechanical stirrer, thermometer and dropping funnel, was added slowly an ethereal solution saturated with hydrogen chloride (6 mL) at room temperature, under a nitrogen atmosphere, with stirring. After about 0.5 hrs at room temperature, the precipitate was collected, washed with anhydrous ether (15 mL) and dried to yield 3.95 g (87.6%) of product.

Provenance & Evidence