Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Iodide → p-Benzyloxybenzyl iodide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Iodide | HCID 5238 | — |
| 반응물 | 4-Benzyloxybenzyl chloride | HCID 70042 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | p-Benzyloxybenzyl iodide | HCID 11723738 | — |
반응 단계
A solution of 1.0 g (4.3 mmol) of 4-benzyloxybenzyl chloride (Fluka; Buchs/Switzerland) in 8 ml of acetone is stirred at RT with 3.13 g (20.9 mmol) of sodium iodide. According to a gas chromatrogram, the reaction is complete after 90 min. Working up as described in Example 21 F) 1) a) yields the title compound: 1H-NMR (200 MHz, CDCl3 : 4.48 (s, 2 H), 5.06 (s, 2 H), 6.85-6.95 (m, 2 H), 7.25-7.48 (m, 7 H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05643878 |
| 출처 데이터셋 | uspto-grants-1997_07 |
| ORD ID | ord-6765b01fadac47acb2bd08c124dbeb97 |
| 출처 메모 | uspto-grants-1997_07 |