Potassium peroxymonosulphate → HCID 88381447, compound

HRID 263799Notes

Reaction equation

HRID 263799 reaction equation
C[O:2][C:3](=[O:5])[CH3:4].[C:6]([OH:14])(=S)[CH2:7][O:8][CH2:9]C(O)=O.[S:15]([O-:20])(O[O-])(=O)=[O:16].[K+].[K+]>CO.O>[CH3:9][O:8][C:7](=[S:15](=[O:20])=[O:16])[CH2:6][O:14][CH2:4][C:3]([OH:2])=[O:5]

Participants

4

Reactant 2

HCID 10313463Potassium peroxymonosulphateHCID 178496526HCID 178496526, compound

Product 1

HCID 88381447HCID 88381447, compound

Reagents, catalysts & solvents 1

HCID 22242641Methanol--water (1/1)Solvent

Procedure

Thiodiglycolic acid monomethyl ether (Indian J. Chem. 25B, 880 (1986)) in a methanol/water mixture is oxidised with potassium peroxomonosulfate at approximately 25° C. to yield the title compound, which is further used.

Sources & evidence

ORD record
ord-820cda0ba78c461e92761a4f13c7e9f1
Source dataset
uspto-grants-1997_07
Patent number
US05643878

Reaction notes

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