HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromophenol → 4-Bromo-2-fluoro-1-(methoxymethoxy)benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromophenol | HCID 7808 | — |
| Reactant | 4-Bromo-2-fluorophenol | HCID 2724981 | — |
| Reactant | 2,3-Difluorobiphenyl-4'-yl acrylate | HCID 21459496 | — |
| Product | 4-Bromo-2-fluoro-1-(methoxymethoxy)benzene | HCID 22032015 | 86.4% |
Reaction Steps
The same procedure as in the synthesis (a) of Example 1 was repeated except that 43.9 g of 2-fluoro-4-bromophenol were used instead of 40 g of p-bromophenol to give 46.7 g (Y., 86.4%) of methoxymethy 4-bromo-2-fluorophenyl ether. GC; 97.2% b.p.; 118°-120° C./14 mmHg
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05645760 |
| Source dataset | uspto-grants-1997_07 |
| ORD ID | ord-e71ccd915d144794817df309de4f5656 |
| Source note | uspto-grants-1997_07 |