HuagongsheHuagongshe Chemistry Print Report · For research reference only
Salicylaldehyde → o-(Allyloxy)benzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Salicylaldehyde | HCID 6998 | — |
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 53427792 | HCID 53427792 | — |
| Product | o-(Allyloxy)benzaldehyde | HCID 101335 | — |
Reaction Steps
Synthesis of formazan monomer used copolymers E34, E35, E36, E37 of table 1, infra. ##STR6## Potassium carbonate (24.0 g, 173.9 mmol) was added to an ethanolic solution containing salicylaldehyde (19.0 g, 155.7 mmol) an allyl bromide (22.0 g, 181.8 mmol). The resulting suspension was heated to reflux overnight. The precipitated inorganic salt was filtered off. The filtrate was evaporated under reduced pressure to give the desired product, 2-allyloxy-benzaldehyde.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05645910 |
| Source dataset | uspto-grants-1997_07 |
| ORD ID | ord-f2eaa7e278d64637b1f79614310311c4 |
| Source note | uspto-grants-1997_07 |