4-Fluorobenzaldehyde → HCID 10068863, compound

HRID 263989Notes

Reaction equation

HRID 263989 reaction equation
[S:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[C:2]1[N:10]([CH2:18][CH2:19][OH:20])[CH2:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1.F[C:22]1[CH:29]=[CH:28][C:25]([CH:26]=[O:27])=[CH:24][CH:23]=1>>[S:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[C:2]1[N:10]([CH2:18][CH2:19][O:20][C:22]1[CH:29]=[CH:28][C:25]([CH:26]=[O:27])=[CH:24][CH:23]=1)[CH2:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

Participants

3

Reactant 2

HCID 680234-FluorobenzaldehydeHCID 10469125HCID 10469125, compound

Product 1

HCID 10068863HCID 10068863, compound

Procedure

The title compound was prepared from 2-(N-(2-benzothiazolyl)-N-benzylamino)ethanol (8.25 g) and 4-fluorobenzaldehyde (3.6 g) by an analogous procedure to that described in Preparation 22.

Workup

  1. customthat described in Preparation 22

Sources & evidence

ORD record
ord-090f9726c7104f16acd3422f00dacd90
Source dataset
uspto-grants-1997_07
Patent number
US05646169

Reaction notes

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