Potassium Hydroxide → HCID 21469573, compound

HRID 264053Notes

Reaction equation

[CH2:1]([N:13]1[C:17]([CH2:18][CH2:19][C:20]([O:22]C)=[O:21])=[N:16][N:15]=[N:14]1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[OH-].[K+]>>[CH2:1]([N:13]1[C:17]([CH2:18][CH2:19][C:20]([OH:22])=[O:21])=[N:16][N:15]=[N:14]1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

Participants

Reactant 2

HCID 14797Potassium Hydroxide

HCID 10639731HCID 10639731, compound

Product 1

HCID 21469573HCID 21469573, compound

Procedure

In a manner similar to Example 34, methyl 1-dodecyl-1H-tetrazole-5-propanoate was saponified with KOH to give 1-dodecyl-1H-tetrazole-5-propanoic acid. The acid was condensed with 2,4,6-trimethoxyaniline to give the title compound, mp 57°-61° C.

Sources & evidence

ORD record: ord-b38d420c5ba24f3cb4e5426957177ee9
Source dataset: uspto-grants-1997_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05646170

Reaction notes

Loading…