Ethyl phenylacetate → HCID 10523008, compound

HRID 264126Notes

Reaction equation

[C:1]1([CH2:7][C:8]([O:10][CH2:11][CH3:12])=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:13][CH:14]([C:16]1[CH:21]=[CH:20][CH:19]=[C:18]([CH:22]([CH3:24])[CH3:23])[C:17]=1[N:25]=[C:26]=[O:27])[CH3:15]>>[CH2:11]([O:10][C:8](=[O:9])[CH:7]([C:26]([NH:25][C:17]1[C:16]([CH:14]([CH3:13])[CH3:15])=[CH:21][CH:20]=[CH:19][C:18]=1[CH:22]([CH3:24])[CH3:23])=[O:27])[C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)[CH3:12]

Participants

Reactant 2

HCID 7590Ethyl phenylacetate

HCID 922592,6-Diisopropylphenyl isocyanate

Product 1

HCID 10523008HCID 10523008, compound

Procedure

In a manner similar to Example 134, phenylacetic acid, ethyl ester was condensed with 2,6-bis(1-methylethyl)phenyl isocyanate to give the title compound, mp 168°-170° C.

Sources & evidence

ORD record: ord-871057f77cfa41f98ad177c01d9977fa
Source dataset: uspto-grants-1997_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05646170

Reaction notes

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