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HRID264333

反应详情

EQUATION

反应方程式

HRID 264333 的结构方程式

REACTANTS

反应物

3
结构：Cl.NOCc1ccccc1
HCID102312

Hydroxylamine, O-benzyl-, hydrochloride

C7H10ClNO

结构：CC(C)(C)ON.Cl
HCID2777906

O-tert-Butylhydroxylamine hydrochloride

C4H12ClNO

结构：COc1ccc(S(=O)(=O)N(Cc2cccnc2)[C@@H](C(=O)O)C(C)C)cc1.Cl
HCID70061703

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc(S(=O)(=O)N(Cc2cccnc2)[C@@H](C(=O)NOCc2ccccc2)C(C)C)cc1
HCID22856293

未命名化合物

PROCEDURE

实验过程

2(R)-[[4-methoxybenzenesulfonyl](3-picolyl)amino]-3-methylbutanoic acid hydrochloride is reacted with O-benzylhydroxylamine hydrochloride under conditions described for reaction with O-t-butylhydroxylamine hydrochloride to yield N-(benzyloxy)-2(R)-[[4-methoxybenzenesulfonyl](3-picolyl)amino]-3-methyl-butanamide, m.p. 74.5°-76° C.