HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 57256727, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 57028147 | HCID 57028147 | — |
| Product | HCID 57256727 | HCID 57256727 | — |
Reaction Steps
128 mg (0.225 mmol) of (2R*,4S*)-2-benzyl-1-(4-quinolylmethyl)-N-(4-quinolylmethyl)-N-trifluoroacetyl-4-piperidinamine are reacted with 34 mg (0.872 mmol) of sodium borohydride in analogy to Example 2. The title compound ##STR39## is obtained as yellow oil. TLC: methylene chloride/methanol/conc. ammonia (700:50:1) Rf =0.45, FD-MS: M+ =490.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05646144 |
| Source dataset | uspto-grants-1997_07 |
| ORD ID | ord-dc8b838c7b0a4d57b82cafb26b583205 |
| Source note | uspto-grants-1997_07 |