Sodium borohydride → HCID 57094336, compound

Participants

Reaction Steps

128 mg (0.218 mmol) of (2R *,4S*)-2-benzyl-1-(2,4-dichlorobenzyl)-N-(4-quinolylmethyl)-N-trifluoroacetyl-4-piperidinamine are reacted with 34 mg (0.920 mmol) of sodium borohydride in analogy to Example 2. The title compound ##STR40## is obtained as yellow oil. TLC: methylene chloride/methanol/conc. ammonia (700:50:1) Rf =0.25, FD-MS: M+ =472.

Provenance & Evidence