HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → HCID 20296415, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | GNF-Pf-3174 | HCID 410965 | — |
| Reactant | HCID 20296434 | HCID 20296434 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 20296415 | HCID 20296415 | — |
Reaction Steps
3-(2-dimethylaminoethoxy)-10-benzyl-9(10H)-acridinone [IV; R' is C6H5CH2, R" is H, --O--Y--N=Z is 3--O--CH2CH2N(CH3)2 ], m.p. 134°-136° C. (light yellow powder). The intermediate 3-chloro-10-benzyl-9(10H)-acridinone, m.p. 186°-190° C. (yellow crystals) was prepared from 3-chloro-9(10H)-acridinone and benzyl bromide with sodium hydride in dimethylformamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04150134 |
| Source dataset | uspto-grants-1979_04 |
| ORD ID | ord-8b3942a0c8564b7ba8398b09d967d53d |
| Source note | uspto-grants-1979_04 |