HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane methanol → HCID 70049736, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane methanol | HCID 21226129 | — |
| Reactant | HCID 86751052 | HCID 86751052 | — |
| Product | HCID 70049736 | HCID 70049736 | — |
Reaction Steps
Analogously to Example 1, the title compound is prepared starting from 66 mg of 5(S)-tert-butoxycarbonylamino-4(S)-hydroxy-7(S)-isopropyl-2(R)-methyl-8-[3,4-di(3-methoxypropyloxy)phenyl]-octanoic acid (N-butyl)amide. This yields the tide compound: Rf (dichloromethane/methanol=9:1)=0.21; Rt (I)=40.0 minutes; FAB-MS (M+H)+ =539.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05646143 |
| Source dataset | uspto-grants-1997_07 |
| ORD ID | ord-49a42c9c1c7e47a4aa2561a0e97b65c8 |
| Source note | uspto-grants-1997_07 |