HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → 2,11-dihydro-11-methyl-3H-s-triazolo[3,4-b][3]benzazepin-3-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 11-Methyl-3-methylthio-11H-s-triazolo[3,4-b][3]benzazepine | HCID 21323534 | — |
| Product | 2,11-dihydro-11-methyl-3H-s-triazolo[3,4-b][3]benzazepin-3-one | HCID 21323347 | — |
Reaction Steps
11-Methyl-3-methylthio-11H-s-triazolo[3,4-b][3]benzazepine was treated with potassium hydroxide and the reaction mixture was treated as described. By this procedure was obtained 2,11-dihydro-11-methyl-3H-s-triazolo[3,4-b][3]benzazepin-3-one as crystals. Pale brown needles (as recrystallized from ethanol), m.p. 119°-120° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04150139 |
| Source dataset | uspto-grants-1979_04 |
| ORD ID | ord-eaa933cba8a54ad894e6426fc27382a7 |
| Source note | uspto-grants-1979_04 |