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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 26513Generated: October 28, 2026

m-Chloroperbenzoic acid → 8-methyl-3-methylsulfinyl-11H-s-triazolo[3,4-b][3]benzazepine

https://huagongshe.com/reaction/26513

Reaction equation

Participants

RoleNameHCIDCharge
Reactantm-Chloroperbenzoic acidHCID 70297—
Reactant8-methyl-3-methylthio-11H-s-triazolo[3,4-b][3]benzazepineHCID 21323337—
Product8-methyl-3-methylsulfinyl-11H-s-triazolo[3,4-b][3]benzazepineHCID 21323374—

Reaction Steps

By a procedure similar to that described in Example 17, 8-methyl-3-methylthio-11H-s-triazolo[3,4-b][3]benzazepine was reacted with m-chloroperbenzoic acid to obtain 8-methyl-3-methylsulfinyl-11H-s-triazolo[3,4-b][3]benzazepine. Colorless needles (as recrystallized from methanol), m.p. 158°-159° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04150139
Source datasetuspto-grants-1979_04
ORD IDord-4a0886c085954195b57c67a493103931
Source noteuspto-grants-1979_04