HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → 8-chloro-3-methylsulfinyl-11H-s-triazolo[3,4-b][3]benzazepine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | 8-chloro-3-methylthio-11H-s-triazolo[3,4-b][3]benzazepine | HCID 21323547 | — |
| Product | 8-chloro-3-methylsulfinyl-11H-s-triazolo[3,4-b][3]benzazepine | HCID 21323333 | — |
Reaction Steps
By a procedure similar to that described in Example 17, 8-chloro-3-methylthio-11H-s-triazolo[3,4-b][3]benzazepine was reacted with m-chloroperbenzoic acid to obtain 8-chloro-3-methylsulfinyl-11H-s-triazolo[3,4-b][3]benzazepine. Colorless needles (as recrystallized from methanol), m.p. 183°-185° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04150139 |
| Source dataset | uspto-grants-1979_04 |
| ORD ID | ord-05ba0d03e464488d9512763ed6ecce82 |
| Source note | uspto-grants-1979_04 |